Summary Single Crystal Synthesis Structure and Magnetism arxiv.org
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This summary highlights the synthesis, structure, and magnetism of single crystals of Pb10-xCux(PO4)6O, focusing on overcoming challenges related to structural defects and impurity phases found in polycrystalline samples.
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Slide Presentation (9 slides)
Key Points
- Superconductivity claim in Pb10-xCux(PO4)6O difficult to confirm due to structural defects and impurity phases in polycrystalline samples
- Synthesis, structure, and magnetism of Pb10-xCux(PO4)6O single crystals analyzed using CrysAlis(Pro) and refined using Olex2 with SHELX
- XRD analysis reveals crystal structure in the P6 3/m space group for Pb9Cu(PO4)6O with refined atomic coordinates
- SEM image and EDX map show spatial distribution of Cu intensity in single crystals
- Magnetization of single crystals measured at different temperatures and magnetic fields, revealing diamagnetism
- Pb10-xCux(PO4)6O5 single crystals grown using TSFZ method and highly insulating
- Phonon bands, localized flat band magnetism, models, and chemical analysis explored in Pb10-xCux(PO4)6O13 single crystal synthesis
Summaries
25 word summary
This summary discusses the synthesis, structure, and magnetism of single crystals of Pb10-xCux(PO4)6O, addressing challenges posed by structural defects and impurity phases in polycrystalline samples.
30 word summary
This summary provides information about the synthesis, structure, and magnetism of single crystals of Pb10-xCux(PO4)6O. The presence of structural defects and impurity phases in polycrystalline samples has made it difficult
190 word summary
A recent claim of superconductivity in Pb10-xCux(PO4)6O has generated interest, but the presence of structural defects and impurity phases in polycrystalline samples has made it difficult to confirm. To address
The document discusses the synthesis, structure, and magnetism of Pb10-xCux(PO4)6O single crystals. The data was analyzed using CrysAlis(Pro) and refined using Olex2 with SHELX. Energy
This text excerpt provides information about the single crystal synthesis, structure, and magnetism of Pb9Cu(PO4)6O. The XRD analysis reveals the crystal structure in the P6 3/m space group, with refined atomic coordinates and
The text excerpt discusses the synthesis, structure, and magnetism of single crystals. The SEM image and corresponding EDX map show the spatial distribution of Cu intensity. The magnetization of the crystals is measured at different temperatures and magnetic fields, revealing a diam
The text excerpt discusses the synthesis, structure, and magnetism of single crystals of Pb10-xCux(PO4)6O5. The crystals were grown using the TSFZ method and are highly insulating. The transport anomalies previously observed
This document discusses the single crystal synthesis, structure, and magnetism of Pb10-xCux(PO4)6O13. The authors explore the phonon bands, localized flat band magnetism, models, and chemical analysis of this compound.